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- W1967352057 abstract "The atomic positions in the crystal structures of anhydrous calcium hydrogen phosphate and monocalcium phosphate monohydrate, described by MacLennan and Beevers (1955, 1956), have been refined by the method of least squares, with allowance for anisotropic thermal vibrations. For monetite, CaHPO4, the final value of the disagreement index was 0.148 over 790 reflections, which led to e.s.d.'s of about 0.015 Å for the eight distinct P–O lengths. Three different close O᠁O approaches have been found and attributed to hydrogen bonds. The hydrogen atom in the first phosphate group is thought to be attached to oxygen O1; in the second, the hydrogens are probably distributed between O7, which has a close approach across a symmetry centre to O7′ of 2.436 ± 0.028 Å, and O6. Nuclear magnetic-resonance spectra are broader than reported previously and do not require the postulation of a change in the structure with temperature." @default.
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- W1967352057 date "1961-11-01" @default.
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- W1967352057 title "The crystal structures of two calcium orthophosphates: CaHPO<sub>4</sub>and Ca(H<sub>2</sub>PO<sub>4</sub>)<sub>2</sub>· H<sub>2</sub>O" @default.
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- W1967352057 doi "https://doi.org/10.1524/zkri.1961.116.1-2.101" @default.
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