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- W1967405902 endingPage "7074" @default.
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- W1967405902 abstract "This report describes a new synthetic approach to symmetrical diamino-substituted Tröger's base analogues, allowing the synthesis of 1,7-, and 4,10-diamino derivatives with no additional substituents and of 3,9-diamino derivative with methyl groups in the 1-, 4-, 7- and 10-positions. The synthesis uses regioselective nitration of dihalo-substituted- or tetrahalo-substituted Tröger's bases followed either by hydrogenation of the nitro functions accompanied by removal of halogen atoms or alternatively by chemoselective reduction of nitro groups to obtain the dihalo-diamino-substituted Tröger's base analogues. The 2,8-diamino derivatives, not accessible by this approach, can be prepared by Buchwald–Hartwig amination of the 2,8-dibromo-substituted Tröger's bases." @default.
- W1967405902 created "2016-06-24" @default.
- W1967405902 creator A5050065720 @default.
- W1967405902 creator A5053743446 @default.
- W1967405902 date "2012-11-15" @default.
- W1967405902 modified "2023-09-25" @default.
- W1967405902 title "Synthesis of Symmetrical Dinitro- and Diamino-Substituted Tröger's Base Analogues" @default.
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- W1967405902 doi "https://doi.org/10.1002/ejoc.201201188" @default.
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