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• W1967528324 abstract "Two-step one-pot reaction conditions have been developed for synthesizing 1-substituted-1,2,3-triazoles. This transformation involves the base-catalyzed deprotection of trimethylsilylacetylene followed by Cu-catalyzed Huisgen 1,3-dipolar cycloaddition under aqueous reaction conditions. Utilization of potassium carbonate as the base and methanol as the alcoholic aqueous co-solvent resulted in optimal yields of the desired products. The reaction conditions were found to be successful for both alkyl and aryl azide reactants, including analogs with electron-donating and electron-withdrawing functionality. This procedure stands as a simple and regioselective means by which to prepare 1-substituted-1,2,3-triazole compounds directly from azide precursors." @default.
• W1967528324 created "2016-06-24" @default.
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• W1967528324 creator A5057554359 @default.
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• W1967528324 date "2008-12-01" @default.
• W1967528324 modified "2023-09-24" @default.
• W1967528324 title "Monosubstituted 1,2,3-triazoles from two-step one-pot deprotection/click additions of trimethylsilylacetylene" @default.
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• W1967528324 doi "https://doi.org/10.1016/j.tetlet.2008.09.136" @default.
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