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- W1967786319 abstract "Refluxing the oxo-alkoxo complexes ReO(OR)Cl 2 py 2 (where RCH 3 and C 2 H 5 ) in toluene yielded an oxo-bridged dinuclear compound {OReCl 2 py 2 } 2 O, in which a transtrans arrangement of pyridien and chloride ligands around rhenium was determined by an X-ray diffraction study. This compound contains the same linear OReReO backbone as the cis,cis isomer first prepared by Wlikinson's group, and the two ReCl 2 N 2 planes are rotated with respect to each other by 27° about the backbone axis. Both stereoisomers are green, they exhibit very similar infrared and 13 C NMR spectra, but they can be distinguished from their 1 H NMR chemical shifts. An X-ray diffraction study on ReO(OCH 3 )Cl 2 py 2 showed the presence of a trans,trans octahedral geometry around the metal and a bent ReOCh 3 group (156°)." @default.
- W1967786319 created "2016-06-24" @default.
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- W1967786319 date "1998-10-01" @default.
- W1967786319 modified "2023-09-26" @default.
- W1967786319 title "Synthesis and crystal structure of a new isomer of the μ-oxo-bis[dichlorooxobis(pyridine)rhenium(V)] complex {OReCl2py2}2O" @default.
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- W1967786319 doi "https://doi.org/10.1016/s0020-1693(98)00111-x" @default.
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