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- W1967797395 abstract "Thermogravimetric measurements were made on NiO from 800° to 1100°C over the oxygen pressure range 10−1 to 10−4 atm. On the basis of complementary conductivity measurements showing a P(O2)1/5 oxygen pressure dependence, it is proposed that the predominant defects are described by an electroneutrality condition involving doubly ionized metal vacancies, impurities, and electron holes, 2[V”M]=[FM]+p. It is shown that for this defect model, the weight change relative to a low oxygen pressure reference weight is a measure of the effective vacancy concentration, defined as [V”M]eff≡[V”M]-≡[FM], and therefore has the same oxygen pressure dependence as the electron hole concentration followed in the conductivity measurements. The expression [V”M]eff=0.168 P(O2)1/5 exp (−0.86±0.15/kT) is derived to express the effective vacancy concentration in NiO. The probable effective impurity content of the specimens used is calculated." @default.
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- W1967797395 date "1970-10-01" @default.
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- W1967797395 title "Gravimetric Determination of Defect Concentrations in NiO" @default.
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- W1967797395 doi "https://doi.org/10.1111/j.1151-2916.1970.tb15958.x" @default.
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