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• W1968124313 endingPage "11286" @default.
• W1968124313 startingPage "11279" @default.
• W1968124313 abstract "First-derivative electron paramagnetic resonance (EPR) absorption spectra of the vanadyl ion (VO2+) in glasses of five different organic−aqueous cosolvent mixtures at 10 K are reported over the 9.4−376 GHz microwave frequency range. Whereas absorption features arising from the g-parallel and g-perpendicular components of the ge tensor are overlapping at low frequencies, it is shown that they are completely separated at microwave frequencies >110 GHz. The analysis of the EPR spectra revealed that line-broadening is due to g-strain over the 9.4−376 GHz range. EPR spectra of VO2+ bound to bovine transferrin in a 1:1 molar ratio were also compared at 9.4 and 110 GHz. The results for the VO2+−transferrin complex showed that absorption features corresponding to the g-parallel and g-perpendicular components of the ge tensor were similarly separated at high frequency and that line-broadening was attributable to g-strain. We show that line-broadening characteristic of g-strain under conditions of low g-anisotropy can be explained by an S = 1/2 spin system in which the principal g values are themselves the random variables described by a normal distribution. On this basis, it is shown that line-broadening is proportional to the microwave frequency and the spread of each of the principal values of the ge tensor." @default.
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• W1968124313 date "1999-12-01" @default.
• W1968124313 modified "2023-10-13" @default.
• W1968124313 title "High-Frequency Electron Paramagnetic Resonance Studies of VO²⁺ in Low-Temperature Glasses" @default.
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• W1968124313 doi "https://doi.org/10.1021/jp991287t" @default.
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