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- W1968132016 abstract "A wide range of five- and six-membered sultams bearing an α-ethoxycarbonyl-α-methyl substituent or an α-aryl group (17 examples) were synthesized by the cyclodialkylation of α-substituted methanesulfonanilides with α,ω-dihaloalkanes in the presence of K2CO3 or under phase-transfer catalysis (PTC) conditions. Upon treatment with K2CO3 in N,N-dimethylformamide (DMF) or NaH in dimethyl sulfoxide (DMSO), N-(2,3-dibromopropyl)-α-toluenesulfonanilides furnished different 1,3-diaryl-2-thia-3-azabicyclo[3.1.0]hexane 2,2-dioxides in good to excellent yields (51–88 %, 16 examples). The 4-methoxyphenyl (PMP) group was easily removed from the sultam nitrogen atom by treatment of the corresponding bicyclic sultams with cerium(IV) ammonium nitrate in acetonitrile (71–84 % yield, 6 examples)." @default.
- W1968132016 created "2016-06-24" @default.
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- W1968132016 date "2012-08-03" @default.
- W1968132016 modified "2023-09-27" @default.
- W1968132016 title "Access to a Wide Range of Sultams by Cyclodialkylation of α-Substituted Methanesulfonanilides" @default.
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- W1968132016 doi "https://doi.org/10.1002/ejoc.201200670" @default.
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