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- W1968164018 abstract "Bei der Umsetzung von Na3AsS4 mit Tetraphenylphosphoniumchlorid in Ethanol oder Dimethylformamid tritt eine intramolekulare Redoxreaktion ein, bei der (PPh4)2As2S6 entsteht. Nach der Röntgenstrukturanalyse (4071 beobachtete Reflexe, R = 7,0%) besteht das Anion aus einem sechsgliedrigen Ring aus zwei As und vier S-Atomen in Sesselkonformation; die beiden As-Atome nehmen die Stellungen 1 und 3 ein und tragen jeweils noch ein terminales Schwefelatom. The Cyclic Thioarsenate(III) (PPh4)2As2S6 The reaction of Na3AsS4 with tetraphenylphosphonium chloride in ethanol or dimethylformamide proceeds with an intramolecular redox reaction, yielding (PPh4)2As2S6. According to its X-ray crystal structure analysis (4071 reflections, R = 0.070) the anion consists of a six-membered ring of two As and four S atoms in the chair conformation. The As atoms occupy the ring positions 1 and 3, and each of them has an additional terminal S atom." @default.
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- W1968164018 date "1995-06-01" @default.
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- W1968164018 title "Das cyclische Thioarsenat(III) (PPh4)2As2S6" @default.
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