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- W1968489452 abstract "Abstract An improved practical synthesis of liquid crystals of trans‐cyclohexyltolans by Sonogashira cross‐coupling reaction of 1‐iodo‐4‐(trans‐4‐alkylcyclohexyl)benzene with aromatic terminal alkynes in the presence of Pd/C (palladium on activated carbon) as low as 0.03 mol% of Pd and CuI (2 mol%) in a mixture solvent of acetone–water (5:2 in volume) is described. The liquid crystals could be obtained in high yields as a solid with excellent purity by simple filtration, and the filtrate could be reused several times while still retaining high catalytic activity. Copyright © 2010 John Wiley & Sons, Ltd." @default.
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- W1968489452 date "2010-03-22" @default.
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- W1968489452 title "An improved practical Pd/C-catalyzed Sonogashira cross-coupling reaction for the synthesis of liquid crystals of trans-cyclohexyltolans" @default.
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- W1968489452 doi "https://doi.org/10.1002/aoc.1642" @default.
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