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- W1968652099 abstract "Nano flower of a new discrete Pb (II) coordination compound, [Pb(pcih)2] (1), (pcih = 2-pyridinecarbaldehyde isonicotinoylhy-drazonate), have been synthesized by a sonochemical process and characterized by scanning electron microscopy (SEM), X-ray diffraction (XRD), FT-IR spectroscopy and elemental analyses. Structural determination of compound 1 reveals the Pb (II) ion is six coordinated, bonded to four nitrogen and two oxygen atoms from two “pcih” ligands. Through strong π–π interactions, the overall structure of 1 is 1D supramolecular chain and with other directional intermolecular interactions, it is further extended into a three dimensional (3D) supramolecular structure. Density functional theory calculations (B3LYP functional) have been performed on complex 1 to provide a qualitative theoretical interpretation of their structural parameters, charge distributions and IR spectra. PbO nanoparticles are obtained by thermolysis of 1 at 180 °C with oleic acid as a surfactant." @default.
- W1968652099 created "2016-06-24" @default.
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- W1968652099 date "2014-11-01" @default.
- W1968652099 modified "2023-09-30" @default.
- W1968652099 title "From discrete to infinite 3D coordination polymer: Sonochemical syntheses and structural characterization of a new nano flower lead (II) coordination compound" @default.
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- W1968652099 doi "https://doi.org/10.1016/j.molstruc.2014.08.019" @default.
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