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- W1968705877 abstract "The interaction between secondary aliphatic amines, R2NH (R = Et, Prn, Pri, Bun, Bui, Bus, n-hexyl, 2-ethylhexyl, cyclohexyl, benzyl, allyl; or R2NH = pyrrolidine) and cupric bromide and/or chloride is described. All the bases afforded 2:1 adducts except those amines branched in the α-position (i.e. R = Pri, Bus, cyclohexyl), with which aminolysis and oxidation-reduction occurred. Pyrrolidine with cupric chloride afforded a 3:1 adduct, the formation of which is ascribed to the small steric requirements of this amine. Thermal decomposition of the bis(amine) complexes resulted in the evolution of the parent secondary amine and formation of diamagnetic materials of indeterminate composition, but containing the dialkylammonium grouping. Infra-red (4000-170 cm−1) spectroscopic and magnetic data are presented." @default.
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- W1968705877 date "1969-01-01" @default.
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- W1968705877 title "The preparation, properties, and infra-red spectra (4000-170 cm−1) of dialkylamine complexes of cupric halides" @default.
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- W1968705877 doi "https://doi.org/10.1016/0022-1902(69)80059-x" @default.
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