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- W1968864619 abstract "The reaction of ethoxyxcarbonyl isothiocyanate with water in the absence of a solvent has yielded the new compound [EtO2CN=CS2C{N(H)CO2Et}{S2CN(H)CO2Et}] (1) in 76% yield that has been isolated in a crystalline form that con-tains one equivalent of ethoxyxcarbonyl isothiocyanate. Compound 1 can be viewed as an adduct of a dimer of EtO2CN=C=S and the dithiocarbamic acid 2. Compound 1 dissociates in solution to yield 2 and free ethoxyxcarbonyl isothiocyanate. Compound 2 can be isolated chromatog-raphically, but it is slowly oxidized when allowed to stand in the open air to form the thiuram disulfide 3. Compounds 1 and 3 were characterized crystallographically. Compound 1 contains an imino-substituted dithietane ring with a dithiocarbamate substitutent bonded to one of the ring carbon atoms. Compound 3 is a thiuram disulfide which has C2 crystallographic symmetry." @default.
- W1968864619 created "2016-06-24" @default.
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- W1968864619 date "1998-07-01" @default.
- W1968864619 modified "2023-10-14" @default.
- W1968864619 title "Formation of a Stable Adduct of Ethoxycarbonyldithiocarbamic Acid and a Dimer of Ethoxycarbonyl Isothiocyanate" @default.
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- W1968864619 doi "https://doi.org/10.1002/(sici)1099-0682(199807)1998:7<1025::aid-ejic1025>3.0.co;2-v" @default.
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