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• W1968896168 abstract "Abstract The arene–ruthenium complex [Ru(η6-C10H14)(dppf)Cl]PF6 (1) was used as a precursor for the syntheses of the [Ru(η6-C10H14)(dppf)Br]PF6 (2), [Ru(η6-C10H14)(dppf)I]PF6 (3), [Ru(η6-C10H14)(dppf)SnF3]PF6 (4) and [Ru(η6-C10H14)(dppf)Cl][SnCl3]·0.45CH2Cl2 (5) complexes by its reactions with KBr, KI, SnF2 and SnCl2, respectively. All of the compounds were characterized by NMR, IR, 57Fe and 119Sn-Mossbauer spectroscopy, and cyclic voltammetry. The single-crystal X-ray structure analysis of the [Ru(η6-C10H14)(dppf)Cl][SnCl3]·0.45CH2Cl2 complex revealed the expected piano-stool geometry. Cyclic voltammograms of the complexes showed only one quasi-reversible electrochemical process, involving the oxidation of Fe(II) and Ru(II) at the same potential, which was confirmed by exhaustive electrolysis experiments. 57Fe-Mossbauer parameters obtained for the complexes (1–5) were fitted with one doublet corresponding to a site of one iron(II). The 119Sn-Mossbauer parameters of the complex (4) indicate that tin is tetra covalent." @default.
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• W1968896168 date "2012-07-01" @default.
• W1968896168 modified "2023-10-14" @default.
• W1968896168 title "Synthesis and characterization of [Ru(η6-C10H14)(dppf)X][PF6] (X=Cl, Br, I, SnF3) compounds: The X-ray structure of [Ru(η6-C10H14)(dppf)Cl][SnCl3]·0.45CH2Cl2" @default.
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• W1968896168 doi "https://doi.org/10.1016/j.poly.2012.05.002" @default.
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