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- W1969007627 abstract "Bis(dichlormethyl)quecksilber, Hg(CHCl2)2, und die gemischten Alkylverbindungen RHgCHCl2 (mit R = CH3, C2H5) werden nach bekannten Vorschriften aus CH2Cl2, Lithiumbutanid und HgCl2 bzw. CH3HgCl oder C2H5HgCl synthetisiert. Die 1H- und 13C-NMR- sowie die IR- und Ramanspektren der flüssigen Alkyle RHgCHCl2 und des hochschmelzenden Hg(CHCl2)2 werden registriert und ausgewertet. Nach der Röntgenstrukturanalyse kristallisiert Hg(CHCl2)2 in der monoklinen Raumgruppe P21/c mit 4 azentrischen Molekülen in der Elementarzelle (R = 0,046). Spectroscopic and X-Ray Structural Investigations on Dichloromethyl Mercury Compounds Bis(dichloromethyl)mercury, Hg(CHCl2)2, and mixed alkyl compounds RHgCHCl2 (with R = CH3, C2H5) have been synthesized by known methods from CH2Cl2, lithium butanide and HgCl2, CH3HgCl or C2H5HgCl, respectively. The 1H-, 13C-NMR as well as the IR and Raman spectra of the liquid alkyls RHgCHCl2 and the high melting Hg(CHCl2)2 have been measured and assigned. According to the X-ray structure determination Hg(CHCl2)2 crystallizes in the monoclinic space group P21/c with 4 non-symmetric molecules per unit cell (R = 0.046)." @default.
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- W1969007627 date "1994-04-01" @default.
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- W1969007627 title "Spektroskopische und r�ntgenographische Untersuchungen an Dichlormethyl-Quecksilberverbindungen" @default.
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- W1969007627 doi "https://doi.org/10.1002/zaac.19946200407" @default.
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