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• W1969138565 endingPage "306" @default.
• W1969138565 startingPage "300" @default.
• W1969138565 abstract "We report our electrochemical studies in a W/O microemulsion phase consisting of a ternary mixture of water, Triton X-100, and toluene. The microemulsion phase plays the dual role of a template in the electrodeposition of nickel and as an electrolytic medium in the study of electron-transfer kinetics. The nickel electrodeposits obtained using this microemulsion phase as a template were characterized by surface analysis techniques such as scanning electron microscopy (SEM) and X-ray diffraction (XRD) studies while cyclic voltammetry (CV) was used to determine the electro-active true surface area of the template-deposited nickel. For electron-transfer studies, CV and electrochemical impedance spectroscopy were employed using potassium ferro/ferricyanide as a redox probe. In contrast to the diffusion-controlled process of the redox probe in aqueous medium, a charge-transfer control was observed in the W/O microemulsion phase. We found that the rate constant value for this particular redox reaction in the microemulsion phase is decreased by about four orders of magnitude when compared to the corresponding value in aqueous medium. The observed phenomenon has been correlated to the structure of the W/O microemulsion phase at the interface, exhibiting a microelectrode array behavior." @default.
• W1969138565 created "2016-06-24" @default.
• W1969138565 creator A5050159821 @default.
• W1969138565 creator A5077782710 @default.
• W1969138565 date "2010-09-01" @default.
• W1969138565 modified "2023-09-25" @default.
• W1969138565 title "Microemulsion phase as a medium for electrodeposition of nickel and electron-transfer study of ferrocyanide–ferricyanide redox system" @default.
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• W1969138565 doi "https://doi.org/10.1016/j.jcis.2010.05.014" @default.
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