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• W1969217441 abstract "The first examples of novel bowl-shaped tribenzotriquinacenes (TBTQs) bearing three dithiametacyclophane units within their arene peripheries are reported. The synthesis is based on a C3v-symmetrical hexakis(chloromethyl)tribenzotriquinacene as the key intermediate and yields the inter-ring metacyclophane-type macrocyclization instead of the intra-ring orthocyclophane-type cyclocondensation. Multiple nucleophilic substitution of the same key intermediate leads to a number of other new 6-fold functionalized tribenzotriquinacenes, some of which may be of interest as readily accessible building blocks for the construction of novel bowl-shaped organic networks. The molecular structures of the novel tris(dithiametacyclophanes) and of the hexakis(chloromethyl)- and hexakis(hydroxymethyl)tribenzo-triquinacenes have been determined by X-ray analysis and interesting host/guest aggregation and torsional effects in the solid state are discussed." @default.
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• W1969217441 date "2007-07-21" @default.
• W1969217441 modified "2023-09-25" @default.
• W1969217441 title "<i>C</i>₃<i>_v</i>-Symmetrical Tribenzotriquinacenes Extended by Six C₁-Functional Groups and the First Triquinacene-Based Tris(dithiametacyclophanes)" @default.
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• W1969217441 doi "https://doi.org/10.1021/jo070565e" @default.
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