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- W1969304612 abstract "Solid-phase synthesis of cyclic head-to-tail peptides using Boc-based protection schemes and side chain anchoring via the β-carboxyl of Asp can lead to substantial levels of epimerization at the α-carbon of Asp. These problems arise largely from the chemistry used for the incorporation of Boc-Asp(OH)-OFm to the polymer. Several conditions for the attachment of this β-carboxyl to hydroxymethyl or bromomethyl resins have been evaluated, in an attempt to achieve effective, epimerization-free anchorings. The most successful routes involve the use of cesium or zinc salts of Boc-Asp(OH)-OFm." @default.
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- W1969304612 date "1996-06-01" @default.
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- W1969304612 title "Solid phase-mediated cyclization of head-to-tail peptides: Problems associated with side chain anchoring" @default.
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- W1969304612 doi "https://doi.org/10.1016/0040-4039(96)00803-9" @default.
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