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• W1969353214 abstract "Abstract Equipment constructed for phase investigations by differential thermal analysis DTA) is described. The samples, usually 1.5–2.5 g, are in platinum crucibles mounted in a nickel block inside a Kanthal-wired “thermal gradient free” laboratory furnace. The reference material is fired Al 2 O 3 . The temperature and the differential temperature are measured by Pt/Pt 10% Rh thermocouples. The differential thermocouple is immersed directly in the molten salt. The equipment has proved very well suited for phase investigations in molten and solid fluorides, including the detection of solidus curves in systems with solid solubility. A survey of the systems investigated is given. The equipment has also been tried for quantitative measurements. The enthalpies of fusion of the alkali metal cryolites, M 3 AlF 6 , were measured by DTA, and the results are compared with values obtained by calorimetry." @default.
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• W1969353214 date "1973-01-01" @default.
• W1969353214 modified "2023-09-24" @default.
• W1969353214 title "Differential thermal analysis equipment for the study of molt nifluoride equilibria" @default.
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• W1969353214 doi "https://doi.org/10.1016/0040-6031(73)85005-1" @default.
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