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- W1969363035 abstract "The system AlCl3·6H2O/cis-H2CDC/trans-H2CDC/solvent was systematically investigated with high-throughput methods to study the influence of the two 1,4-cyclohexanedicarboxylate isomers (cis- and trans-H2CDC) as flexible aliphatic linker molecules on the formation of new crystalline compounds. Using the cis-isomer, the layered inorganic–organic hybrid compound [Al(OH)(cis-CDC)] (1) is formed. The use of trans-H2CDC leads to the microporous MOF [Al(OH)(trans-CDC)]·H2O (2) denoted CAU-13. Its framework is related to the well-known MIL-53, which was previously described for trivalent cations and rigid terephthalate linker molecules. The crystal structures of 1 and 2 were derived from powder X-ray diffraction data. Temperature-dependent in situ energy dispersive X-ray diffraction (EDXRD) experiments for the synthesis of 2 were carried out at HASYLAB, DESY, Hamburg. The kinetic analysis, applying the Gualtieri model to the experimental data, revealed Arrhenius activation energies of 76 kJ/mol for both the nucleation and the growth process. These values do not differ much from the activation energies reported for MOFs with aromatic rigid linker molecules." @default.
- W1969363035 created "2016-06-24" @default.
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- W1969363035 date "2013-07-17" @default.
- W1969363035 modified "2023-09-27" @default.
- W1969363035 title "Aluminum-1,4-cyclohexanedicarboxylates: High-Throughput and Temperature-Dependent in Situ EDXRD Studies" @default.
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- W1969363035 doi "https://doi.org/10.1021/ic400825b" @default.
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