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- W1969432858 abstract "Abstract Ammonium and methylammonium hexchloroplumbates of general formula [(CN 3 ) n NH 4− n ] 2 PbCl 6 , with n = 0−4, undergo thermal decomposition on heating to 720 K. The thermal processes are studied by differential thermal analysis and thermogravimetry. Isothermal experiments are done in an apparatus which permits a quantitative determination of some of the products. Thermolysis occurs in two steps: (i) liberation of chlorine [(CH 3 ) n NH 4− n ] 2 PbCl 6 (s,l) → PbCl 2 (s) + 2 [(CH 3 ) n NH 4− n ]Cl(s) + Cl 2 (g); (ii) thermal processes which occur on heating the solid products of the above reaction; for compounds with n = 0−3, the process is described by, PbCl 2 (s) + 2 [(CH 3 ) n NH 4− n ] Cl(s) → PbCl 2 (s) + 2(CH 3 ) n NH 3− n (g) + 2 HCl(g). When the second reaction is slow in the temperature range of the first, chlorine is rapidly evolved and stoichiometric amounts discharged at stage (i). If this condition is not satisfied, secondary reaction occur, mostly in the gas phase, which consume chlorine." @default.
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- W1969432858 date "1980-03-01" @default.
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- W1969432858 title "Thermal reactions of lead(IV) chloride complexes in the solid state. Part III. Thermolysis of ammonium and methyl-substituted ammonium hexachloroplumbates" @default.
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- W1969432858 doi "https://doi.org/10.1016/0040-6031(80)87012-2" @default.
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