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• W1969502000 abstract "Abstract Cobalt and chromium K-edge XAFS (X-ray Absorption Fine Structure) spectra of [Co(ox)3[3−, [Co(ox)2]−, [Co(mal)2en]− and [Cr(ox)3]3− (ox = oxalate, mal = malonate, en = ethylenediamine) in solids and in various solvents were measured. XANES (X-ray Absorption Near-Edge-Structure) spectra of a trisoxolato cobalt complex, and a chromium complex, vary with the type of solvent, while such a solvent effect was not detected for [Co(ox)2en]− and [Co(mal)2en]−. EXAFS (Extended X-ray Absorption Fine Structure) analyses of the trisoxalato complexes in solvents indicate that metal-coordinating atom distances vary depending on the solvents used and linear reduction of the distances was observed with increasing Gutmann's acceptor number of a solvent. This trend is apparently in accord with the observed blue shifts in d-d absorption spectra of [Co(ox)3]− in greater acceptor number solvents. Furthermore, it was found that othr metal-ligand atom distances than interatomic distances of metal-directly coordinating atoms also shrink with acceptor numbers of solvents." @default.
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• W1969502000 date "1994-05-01" @default.
• W1969502000 modified "2023-09-27" @default.
• W1969502000 title "Solvent effects on cobalt(III) and chromium(III) oxalato complexes by x-ray absorption fine structure" @default.
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• W1969502000 doi "https://doi.org/10.1016/s0277-5387(00)83458-0" @default.
• W1969502000 hasPublicationYear "1994" @default.
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