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- W1969536472 abstract "Jones oxidation of suitably protected allyl beta-D-galactopyranosides and subsequent esterification were reinvestigated. Partial deprotection of the resulting D-galacturonic acid derivatives afforded compounds suitable for transformation into glycosyl acceptors. The synthesis of 2-, 3-, and 4-trityl ethers, relying on efficient differential protecting-group strategies, is described. Trityl-cyanoethylidene condensation of these trityl ethers, leading to the protected disaccharide units beta-D-GalpA-(1-->2)-D-GalpA and beta-D-GalpA-(1-->3)-GalpA with high stereoselectivity, is demonstrated. A beta-D-GalpA-(1-->4)-D-GalpA disaccharide was also prepared." @default.
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- W1969536472 date "1992-12-01" @default.
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- W1969536472 title "d-Galacturonic acid derivatives as acceptors and donorsin glycosylation reactions" @default.
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- W1969536472 doi "https://doi.org/10.1016/s0008-6215(92)84237-m" @default.
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