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- W1969730059 abstract "The submicroscopic structure of synthetic Hg2Cl2 monocrystals was investigated by means of transmission electron microscopy (TEM), scanning electron microscopy (SEM), indirect imaging of surfaces (Pt/C replica technique) as well as by application of supplementary methods. As already reported by NEUMANN et al., TEM-images show a periodic stripelike contrast whose period varies from 0.1 mm to 0.2 mm. It proved that the stripelike contrast arises from a periodic chemical inhomogeneity of the synthetic crystals. The chemical inhomogeneity probably consists in periodic deviations from the stoichiometric composition of Hg2Cl2. By reason of the orientation on {110}-, (001)-, and {114} faces a reconstruction of arrangement of the structures in the crystals is carried out. According to that, the stripes have to be interpreted as intersection lines of 2-dimensional formations with the corresponding faces.Die submikroskopische Struktur synthetischer Hg2Cl2-Einkristalle wurde mittels Transmissions-Elektronenmikroskopie (TEM), Raster-Elektronenmikroskopie (REM), indirekter Oberflachenabbildung (Pt/C-Schragbeschattung) sowie unter Anwendung erganzender Methoden untersucht. Die TEM-Abbildungen zeigen einen periodischen, streifenartigen Kontrast, wie er schon von NEUMANN et al. gefunden wurde. Die Periode der Streifen betragt 0.1 mm – 0.2 mm. Die Experimente ergaben, das die Ursache des streifenartigen Kontrastes in einer periodischen chemischen Inhomogenitat der synthetischen Kristalle besteht. Die chemische Inhomogenitat wird auf periodische Abweichungen von der stochiometrischen Zusammensetzung des Hg2Cl2 zuruckgefuhrt. Auf Grund der Orientierung auf {110}-, (001)- und {114}-Flachen wird eine Rekonstruktion der Lage der Strukturen in den Kristallen durchgefuhrt. Danach sind die Streifen als Schnittlinien 2-dimensionaler Formationen mit den entsprechenden Flachen zu interpretieren." @default.
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- W1969730059 date "1982-01-01" @default.
- W1969730059 modified "2023-09-28" @default.
- W1969730059 title "Electron Optical Investigation of Growth-Induced Inhomogeneities of Synthetic Hg2Cl2 Monocrystals" @default.
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- W1969730059 doi "https://doi.org/10.1002/crat.2170170405" @default.
- W1969730059 hasPublicationYear "1982" @default.
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