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- W1969788986 abstract "Synthesis of PD 158771 (Figure 1) involved 4-amino-cyclohexylacetic acid and its ethyl ester intermediates which required purification to obtain the desired corresponding trans-isomer. HPLC methods were developed for the separation of cis- and trans-4-aminocyclohexylacetic acid and the corresponding ethyl esters following pre-column derivatization with Nα-(2,4-dinitro-5-fluorophenyl)-L-alaninamide (Marfey's reagent). The chromatographic conditions were varied to achieve optimal separation. HIGH-PERFORMANCE LIQUID CHROMATOGRAPHIC METHOD FOR THE SEPARATION OF ISOMERS OF CIS- AND TRANS-4-AMINOCYCLOHEXYLACETIC ACID AND CORRESPONDING ETHYL ESTERAll authorsN. J. Maddox & S. Linhttps://doi.org/10.1081/JLC-100101738Published online:19 August 2006 Figure 1. Structure of PD 158771. Figure 1. Structure of PD 158771." @default.
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- W1969788986 date "1999-01-01" @default.
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- W1969788986 title "HIGH-PERFORMANCE LIQUID CHROMATOGRAPHIC METHOD FOR THE SEPARATION OF ISOMERS OF<i>CIS</i>- AND<i>TRANS</i>-4-AMINOCYCLOHEXYLACETIC ACID AND CORRESPONDING ETHYL ESTER" @default.
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