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- W1969804709 abstract "Abstract The synthesis and characterization of several mesomorphic copolymer sidechain siloxanes is presented and discussed from the standpoints of the extent of pendant substitution as well as composition. For a given copolymer, both the glass-mesomorphic and mesomorphic-isotropic transition temperatures were found to increase, although not linearly so, with increasing substitution up to ca. 70% extent of reaction (determined by FT-NMR and elemental analysis), beyond which, however, there was then little further change in either. In addition, the glass-mesomorphic transition temperature increased more slowly than that for the mesomorphic-isotropic transition as the copolymer composition was varied. The findings confirm the results reported some time ago that even partially-reacted poly(mesomorph-co-hydro)siloxanes can exhibit liquid-crystalline properties over extensive temperature ranges; as well as the contention that judicious adjustment of the makeup of sidechain siloxanes can provide a variety of materials that are useful both as gas- and liquid-chromatographic stationary phases." @default.
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- W1969804709 date "1987-12-01" @default.
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- W1969804709 title "Probe-Solute Study of Mesomorphic Polysiloxane (MEPSIL) Solvents. Synthesis and Characterization of Some Ester-Linked Copolymer Mepsil Stationary Phases" @default.
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- W1969804709 doi "https://doi.org/10.1080/00268948708074559" @default.
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