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• W1970117105 abstract "A variety of metal tungstates have been synthesised in a microwave assisted oven at100 and 150°C and corresponding autogenous water vapour pressure within a timeframe of 30 minutes to 2 hours. The crystals formed are of submicrometer size andshow equidimensional and needle-like crystals. Increasing the synthesis time andtemperature results in the disappearance of the needles and the growth of theequidimensional crystals. The Raman spectra are consistent with those reported forthe natural equivalents of these tungstates. The lead tungstate ν1(Ag) mode is observedat 904 cm-1, while the ν2(Ag) vibration is observed as a strong band at at 326 cm-1accompanied by a weak ν2(Bg) . at 356 cm-1. The ν3(Bg) vibration is located around741 cm-1, whereas the ν3(Eg) is found at 751 cm-1. Finally, the ν4(Bg) vibration iscompletely overlapping with the ν2(Ag) vibration. The band around 271 cm-1 may bethe equivalent of the infrared active ν4(Au) activated due to strain in the crystal. Thetwo bands at 190 and 177 cm-1 are ascribed to the ν(Pb-O) and as a translational modeof the WO4 group in stolzite." @default.
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• W1970117105 date "2004-12-01" @default.
• W1970117105 modified "2023-09-26" @default.
• W1970117105 title "Microwave-assisted synthesis and characterisation of divalent metal tungstate nanocrystalline minerals: ferberite, hübnerite, sanmartinite, scheelite and stolzite" @default.
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• W1970117105 doi "https://doi.org/10.1016/j.matchemphys.2004.08.013" @default.
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