FRINK Linked Data Fragments server

Matches in SemOpenAlex for { <https://semopenalex.org/work/W1970411432> ?p ?o ?g. }

• W1970411432 endingPage "580" @default.
• W1970411432 startingPage "573" @default.
• W1970411432 abstract "A procedure involving hollow fiber microporous membrane liquid-liquid extraction (HF-MMLLE) and detection by liquid chromatography with tandem mass spectrometry was developed and applied. The extraction is based on liquid-liquid microextraction with a polypropylene porous membrane as a solid support for the solvent. On the membrane walls the solvent forms a renewable liquid membrane which improves the trueness of the method and promotes the sample clean-up. The applicability of this method was evaluated through the simultaneous extraction of 18 pesticides of different classes: polar organophosphates, carbamates, neonicotinoids, amides, pyrimidines, benzimidazoles and triazoles in industrial and fresh orange juice. The parameters affecting the extraction efficiency were optimized by multivariable designs. Under optimized conditions, analytes were concentrated onto 1.5 cm long microporous membranes placed directly into the sample containing 9mL of juice at pH 7.0, 4 g of ammonium sulfate and 400 μL of toluene:ethyl acetate (85:15, v/v). The best extraction conditions were achieved at 25°C with 35 min of extraction time. The analyte desorption was carried out using 50 μL of methanol:acetone (50:50, v/v) for 2 min in an ultrasonic bath. Limits of detection ranging between 0.003-0.33 mgL(-1), 0.003-0.35 mg L(-1) and 0.003-0.15 mgL(-1) were obtained for the carton orange juice, carton light orange juice and fresh orange juice samples, respectively. Good repeatability (lower than 7.6%) was obtained for all three sample types. The method was applied to five different juice samples containing soybean extract, orange pulp, nectar, light juice and fresh orange juice. The results suggest that the proposed method represents a very simple and low-cost alternative microextraction procedure rendering adequate limits of quantification for the determination of these pesticides in juice samples." @default.
• W1970411432 created "2016-06-24" @default.
• W1970411432 creator A5021118979 @default.
• W1970411432 creator A5034073359 @default.
• W1970411432 creator A5079029348 @default.
• W1970411432 date "2012-01-01" @default.
• W1970411432 modified "2023-10-13" @default.
• W1970411432 title "Multiresidue determination of pesticides in industrial and fresh orange juice by hollow fiber microporous membrane liquid–liquid extraction and detection by liquid chromatography–electrospray-tandem mass spectrometry" @default.
• W1970411432 cites W1564926529 @default.
• W1970411432 cites W1977091450 @default.
• W1970411432 cites W1978826998 @default.
• W1970411432 cites W1993076271 @default.
• W1970411432 cites W1996439536 @default.
• W1970411432 cites W2003507098 @default.
• W1970411432 cites W2007811173 @default.
• W1970411432 cites W2008914876 @default.
• W1970411432 cites W2017847224 @default.
• W1970411432 cites W2022508126 @default.
• W1970411432 cites W2024711358 @default.
• W1970411432 cites W2039387052 @default.
• W1970411432 cites W2050414528 @default.
• W1970411432 cites W2063210597 @default.
• W1970411432 cites W2092088336 @default.
• W1970411432 cites W2133597621 @default.
• W1970411432 doi "https://doi.org/10.1016/j.talanta.2011.11.037" @default.
• W1970411432 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/22265543" @default.
• W1970411432 hasPublicationYear "2012" @default.
• W1970411432 type Work @default.
• W1970411432 sameAs 1970411432 @default.
• W1970411432 citedByCount "60" @default.
• W1970411432 countsByYear W19704114322012 @default.
• W1970411432 countsByYear W19704114322013 @default.
• W1970411432 countsByYear W19704114322014 @default.
• W1970411432 countsByYear W19704114322015 @default.
• W1970411432 countsByYear W19704114322016 @default.
• W1970411432 countsByYear W19704114322017 @default.
• W1970411432 countsByYear W19704114322018 @default.
• W1970411432 countsByYear W19704114322019 @default.
• W1970411432 countsByYear W19704114322020 @default.
• W1970411432 countsByYear W19704114322021 @default.
• W1970411432 countsByYear W19704114322022 @default.
• W1970411432 countsByYear W19704114322023 @default.
• W1970411432 crossrefType "journal-article" @default.
• W1970411432 hasAuthorship W1970411432A5021118979 @default.
• W1970411432 hasAuthorship W1970411432A5034073359 @default.
• W1970411432 hasAuthorship W1970411432A5079029348 @default.
• W1970411432 hasBestOaLocation W19704114321 @default.
• W1970411432 hasConcept C119128265 @default.
• W1970411432 hasConcept C162356407 @default.
• W1970411432 hasConcept C178790620 @default.
• W1970411432 hasConcept C185592680 @default.
• W1970411432 hasConcept C2778576202 @default.
• W1970411432 hasConcept C2780471494 @default.
• W1970411432 hasConcept C2992423453 @default.
• W1970411432 hasConcept C31827203 @default.
• W1970411432 hasConcept C31903555 @default.
• W1970411432 hasConcept C43617362 @default.
• W1970411432 hasConcept C4725764 @default.
• W1970411432 hasConcept C86381522 @default.
• W1970411432 hasConceptScore W1970411432C119128265 @default.
• W1970411432 hasConceptScore W1970411432C162356407 @default.
• W1970411432 hasConceptScore W1970411432C178790620 @default.
• W1970411432 hasConceptScore W1970411432C185592680 @default.
• W1970411432 hasConceptScore W1970411432C2778576202 @default.
• W1970411432 hasConceptScore W1970411432C2780471494 @default.
• W1970411432 hasConceptScore W1970411432C2992423453 @default.
• W1970411432 hasConceptScore W1970411432C31827203 @default.
• W1970411432 hasConceptScore W1970411432C31903555 @default.
• W1970411432 hasConceptScore W1970411432C43617362 @default.
• W1970411432 hasConceptScore W1970411432C4725764 @default.
• W1970411432 hasConceptScore W1970411432C86381522 @default.
• W1970411432 hasFunder F4320320997 @default.
• W1970411432 hasFunder F4320322025 @default.
• W1970411432 hasLocation W19704114321 @default.
• W1970411432 hasLocation W19704114322 @default.
• W1970411432 hasOpenAccess W1970411432 @default.
• W1970411432 hasPrimaryLocation W19704114321 @default.
• W1970411432 hasRelatedWork W1950305724 @default.
• W1970411432 hasRelatedWork W1969559554 @default.
• W1970411432 hasRelatedWork W2014605936 @default.
• W1970411432 hasRelatedWork W2023409950 @default.
• W1970411432 hasRelatedWork W2034852243 @default.
• W1970411432 hasRelatedWork W2040912236 @default.
• W1970411432 hasRelatedWork W2060470559 @default.
• W1970411432 hasRelatedWork W2115218143 @default.
• W1970411432 hasRelatedWork W2887446520 @default.
• W1970411432 hasRelatedWork W2938182511 @default.
• W1970411432 hasVolume "88" @default.
• W1970411432 isParatext "false" @default.
• W1970411432 isRetracted "false" @default.
• W1970411432 magId "1970411432" @default.
• W1970411432 workType "article" @default.