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- W1970415265 abstract "Abstract A series of quaternary lanthanum gallium tin antimonides LaGa x Sn y Sb 2 was elaborated to trace the structural evolution between the known end members LaGaSb 2 (SmGaSb 2 -type) and LaSn y Sb 2 (LaSn 0.75 Sb 2 -type). Five members of this series were characterized by single-crystal X-ray diffraction. For low Sn content, the Sn atoms disorder with Ga atoms in zigzag chains to form solid solutions LaGa 1– y Sn y Sb 2 (0≤y≤0.2) adopting the SmGaSb 2 -type structure, as exemplified by LaGa 0.92(3) Sn 0.08 Sb 2 and LaGa 0.80(3) Sn 0.20 Sb 2 (orthorhombic, space group D 5 2 − C 222 1 , Z =4). For higher Sn and lower Ga content, there is a segregation in which the Sn atoms appear in chains of closely spaced partially occupied sites as in the parent LaSn 0.75 Sb 2 -type structure whereas the Ga atoms remain in zigzag chains as in the parent SmGaSb 2 -type structure. This feature is observed in the structures of LaGa 0.68(4) Sn 0.31(3) Sb 2 , LaGa 0.62(3) Sn 0.32(3) Sb 2 , and LaGa 0.43(3) Sn 0.39(3) Sb 2 (orthorhombic, space group D 17 2 h − Cmcm , Z =4). The last example illustrates that the combined Ga/Sn content can be substoichiometric ( x + y 2 ∞ [LaSb 2 ] slabs." @default.
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- W1970415265 date "2002-08-01" @default.
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- W1970415265 title "Lanthanum Gallium Tin Antimonides LaGaxSnySb2" @default.
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- W1970415265 doi "https://doi.org/10.1006/jssc.2002.9616" @default.
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