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• W1970628634 abstract "[Fe(3)(μ(3)-O)(μ-OAc)(6)(py)(3)][FeBr(4)](2)[py·H], complex (1), (OAc is acetate) was prepared from the reaction of FeBr(3) with pyridine in 1.2 molar aqueous HBr and 2.4 molar aqueous CH(3)COOH. Recrystallization of 1 in acetonitrile produced the [Fe(3)(μ(3)-O)(μ-OAc)(6)(py)(3)][FeBr(4)] complex (2). Both complexes were characterized by IR and (1)H NMR spectroscopies and their structures were studied using the single-crystal diffraction method. There is a lack of thorough characterization of the titled compounds in solution. Paramagnetic (1)H NMR is introduced as a good probe for the characterization of a family of titled compounds in solution when the L ligand coordinated to iron varies as: CH(3)OH, CH(3)CN, DMSO, H(2)O, py and acetone." @default.
• W1970628634 created "2016-06-24" @default.
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• W1970628634 date "2012-01-01" @default.
• W1970628634 modified "2023-09-25" @default.
• W1970628634 title "Solution and solid state characterization of oxo-centered trinuclear iron(III) acetate complexes [Fe3(μ3-O)(μ-OAc)6(L)3]+" @default.
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• W1970628634 doi "https://doi.org/10.1016/j.saa.2011.08.034" @default.
• W1970628634 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/22020165" @default.
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