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- W1970660890 abstract "Silver particles have been deposited at externally polarised 1,2-dichloroethane (DCE)/water interfaces supported at the tip of micro- and nanopipettes. The electrochemical process involved the reduction of silver ion in the aqueous phase by an organic-phase electron donor (butylferrocene). The silver nucleation and growth process was investigated using potential step chronoamperometry, and the resulting current–time transients were analysed to extract nucleus numbers. At larger pipettes, with diameters of several micrometers, multi-particle nucleation was observed and optical microscopy provided direct evidence for metal electrodeposition at the liquid/liquid interface. For pipettes with radii of 0.5 μm or smaller, the current–time behaviour was consistent with single particle generation. Under some conditions, detachment of the particle from the liquid/liquid interface was inferred from the current–time characteristics, and it is suggested that controlled-detachment from micropipettes could provide a method for the deposition of small metal structures on surfaces." @default.
- W1970660890 created "2016-06-24" @default.
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- W1970660890 date "2003-12-01" @default.
- W1970660890 modified "2023-10-16" @default.
- W1970660890 title "Formation of mesoscopic silver particles at micro- and nano-liquid/liquid interfaces" @default.
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- W1970660890 doi "https://doi.org/10.1016/j.elecom.2003.09.012" @default.
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