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• W1970912845 abstract "An entire series of Starburst polyamidoamine (PAMAM) dendrimers consisting of generations 1 through 10 (G1–10) have been studied by positive-ion electrospray ionization mass spectrometry (ESI-MS) using an extended m/z range quadrupole mass spectrometer. Charge-state distributions were detected as high as m/z 12 000 for the generation 10 dendrimer, having a theoretical molecular weight of 1 megadalton and containing approximately 93 maximum positive charges on the molecule. Accurate molecular weight determinations of the smaller generation dendrimers (G1–3, Mr ∼ 1.4kDa to 6.9kDa) were obtained using a commercial triple quadrupole instrument. The unit resolution ESI mass spectra provide information on the number of incomplete reactions which may occur during polymer synthesis. The extent of gas-phase charging observed by ESI-MS on the entire series of macromolecules was found to exhibit a linear relationship to M, consistent with theoretical models prediciting a spherical ion structure with maximum charging controlled by Coulombic effects." @default.
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• W1970912845 date "1995-01-01" @default.
• W1970912845 modified "2023-10-09" @default.
• W1970912845 title "Detection of high molecular weight starburst dendrimers by electrospray ionization mass spectometry" @default.
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• W1970912845 doi "https://doi.org/10.1002/rcm.1290091516" @default.
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