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• W1971027326 abstract "[(CH3S)3S]+SbF6-, the first example of a trithiosulfonium salt saturated with organyl groups, was prepared from SH3+SbF6- and CH3SCl and characterized by 1H, 13C NMR, infrared, and Raman spectroscopy. The colorless salt is stable up to 10 °C, but solutions in SO2 decompose at −60 °C in a few hours. The structure of the cation was studied by ab initio calculations and a normal coordinate analysis based on four additional isotopic derivates [(CH334S)3S]+SbF6-, [(CH3S)334S]+SbF6-, [(13CH3S)3S]+SbF6-, and [(CD3S)3S]+SbF6-. The cation possesses C3 symmetry with a pyramidal trithiosulfonium unit with predicted geometry parameters of r(SS) = 208.8 pm and ∠(SSS) = 104.06°." @default.
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• W1971027326 date "2000-01-26" @default.
• W1971027326 modified "2023-09-27" @default.
• W1971027326 title "Synthesis and Characterization of the Tris(methylthio)sulfonium Salt [(CH₃S)₃S]⁺SbF₆^-¹" @default.
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• W1971027326 doi "https://doi.org/10.1021/ja9917518" @default.
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