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- W1971160378 abstract "Abstract Ruthenium–arene complexes that contain either 4-vinylpyridine, an alkylating agent for sulfhydryl groups, or a pentachlorophenol ester, a known acylating agent, have been prepared and characterized by 1 H NMR, IR spectroscopy, and elemental analysis. Neutral complexes (η 6 -C 6 H 6 )Cl 2 (4-vinylpyridine)Ru(II), (η 6 -C 6 H 6 )Cl 2 pentachlorophenylisonicotinateRu(II), and (η 6 -C 6 H 6 )Cl 2 pentachlorophenyl-3-(4-pyridyl)propionateRu(II) were synthesized from the arenedichlororuthenium dimer. Dicationic complexes [(η 6 -C 6 H 6 )(NN)(4-vinylpyridine)Ru(II)](BF 4 ) 2 and [(η 6 -C 6 H 6 )(NN)pentachlorophenylisonicotinateRu(II)](BF 4 ) 2 (where NN = 2,2′-bipyridyl and ethylenediamine) were made from the monocation [(η 6 -C 6 H 6 )(NN)ClRu(II)]BF 4 . These complexes may serve as protein-labeling agents because they contain activated organic ligands which can covalently bind to proteins. Metal-bound ligands modification reactions were performed with the reactive [(η 6 -C 6 H 6 )(NN)pentachlorophenylisonicotinateRu(II)](BF 4 ) 2 and isopropylamine. [(η 6 -C 6 H 6 )(NN)(N-isopropylisonicotinamide)Ru(II)](BF 4 ) 2 was isolated in moderate yield and characterized." @default.
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- W1971160378 date "1985-02-01" @default.
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- W1971160378 title "Preparation of arene ruthenium(II) complexes with activated ligands for protein labeling" @default.
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- W1971160378 doi "https://doi.org/10.1016/s0020-1693(00)86575-5" @default.
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