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• W1971185280 endingPage "2578" @default.
• W1971185280 startingPage "2569" @default.
• W1971185280 abstract "The NaBH4 reduction of a mixture of [Au(PPh3)Cl] and [Rh(CNC8H9)3Cl] leads to a dark red solution containing several Au–Rh cluster compounds, from which [Rh(CNC8H9)3(AuPPh3)5]2+1 and [Rh(CNC8H9)2(AuPPh3)6(AuCl)2]+2 have been isolated. The cluster [Rh(CO)2(AuPPh3)7]2+3 has been synthesised by addition of 1 equivalent of [Au(PPh3)(NO3)] to the tetrahydrofuran-soluble fraction of a solution obtained by the borohydride reduction of a mixture of [Au(PPh3)(NO3)] and [Rh(CO)2(MeCN)2]NO3. Compounds 1 and 3 have been characterised using 31P-{1H} NMR, IR and fast atom bombardment mass spectroscopy and single-crystal X-ray techniques. Since 2 was formed only in low yield it has been characterised only by single-crystal X-ray diffraction methods. The structures of the three compounds are related and may be described as derivatives of a rhodiumcentred Au12 icosahedron formed by removing four, five and seven vertices from the icosahedral cage." @default.
• W1971185280 created "2016-06-24" @default.
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• W1971185280 date "1991-01-01" @default.
• W1971185280 modified "2023-09-26" @default.
• W1971185280 title "Synthesis of heteronuclear gold–rhodium cluster compounds and structural characterisation of [Rh(CNC₈H₉)₃(AuPPh₃)₅]²⁺, [Rh(CNC₈H₉)₂(AuPPh₃)₆(AuCl)₂]⁺and [Rh(CO)₂(AuPPh₃)₇]²⁺" @default.
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• W1971185280 doi "https://doi.org/10.1039/dt9910002569" @default.
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