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• W1971225110 startingPage "2421" @default.
• W1971225110 abstract "Abstract This study aimed to elucidate the structural nature of the polydisperse, nanoscopic components in the solution and the solid states of partially reduced polyoxomolybdate derived from the {Mo 132 } keplerate, {(Mo)Mo 5 } 12 ‐{Mo 2 acetate} 30 . Designer tripodal hexamine‐tris‐crown ethers and nanoscopic molybdate coprecipitated from aqueous solution. These microcrystalline solids distributed particle radii between 2–30 nm as assayed by transmission electron microscopy (TEM). The solid materials and their particle size distributions were snap shots of the solution phase. The mother liquor of the preparation of the {Mo 132 } keplerate after three days revealed large species ( r =20–30 nm) in the coprecipitate, whereas {Mo 132 } keplerate redissolved in water revealed small species (3–7 nm) in the coprecipitate. Nanoparticles of coprecipitate were more stable than solids derived solely from partially reduced molybdate. The TEM features of all material analyzed lacked facets on the nanometer length scale; however, the structures diffracted electrons and appeared to be defect‐free as evidenced by Moiré patterns in the TEM images. Moiré patterns and size‐invariant optical densities of the features in the micrographs suggested that the molybdate nanoparticles were vesicular." @default.
• W1971225110 created "2016-06-24" @default.
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• W1971225110 date "2004-05-07" @default.
• W1971225110 modified "2023-10-12" @default.
• W1971225110 title "Kinetic Precipitation of Solution-Phase Polyoxomolybdate Followed by Transmission Electron Microscopy: A Window to Solution-Phase Nanostructure" @default.
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• W1971225110 doi "https://doi.org/10.1002/chem.200305468" @default.
• W1971225110 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/15146515" @default.
• W1971225110 hasPublicationYear "2004" @default.
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