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• W1971242034 startingPage "6056" @default.
• W1971242034 abstract "A highly sensitive analytical method is required for the assessment of nanomolar perchlorate contamination in drinking water as an emerging environmental problem. We developed the novel approach based on a voltammetric ion-selective electrode to enable the electrochemical detection of redox-inactive perchlorate at a nanomolar level without its electrolysis. The perchlorate-selective electrode is based on the submicrometer-thick plasticized poly(vinyl chloride) membrane spin-coated on the poly(3-octylthiophene)-modified gold electrode. The liquid membrane serves as the first thin-layer cell for ion-transfer stripping voltammetry to give low detection limits of 0.2-0.5 nM perchlorate in deionized water, commercial bottled water, and tap water under a rotating electrode configuration. The detection limits are not only much lower than the action limit (approximately 246 nM) set by the U.S. Environmental Protection Agency but also are comparable to the detection limits of the most sensitive analytical methods for detecting perchlorate, that is, ion chromatography coupled with a suppressed conductivity detector (0.55 nM) or electrospray ionization mass spectrometry (0.20-0.25 nM). The mass transfer of perchlorate in the thin-layer liquid membrane and aqueous sample as well as its transfer at the interface between the two phases were studied experimentally and theoretically to achieve the low detection limits. The advantages of ion-transfer stripping voltammetry with a thin-layer liquid membrane against traditional ion-selective potentiometry are demonstrated in terms of a detection limit, a response time, and selectivity." @default.
• W1971242034 created "2016-06-24" @default.
• W1971242034 creator A5036952838 @default.
• W1971242034 creator A5091326253 @default.
• W1971242034 date "2008-07-10" @default.
• W1971242034 modified "2023-09-23" @default.
• W1971242034 title "Stripping Analysis of Nanomolar Perchlorate in Drinking Water with a Voltammetric Ion-Selective Electrode Based on Thin-Layer Liquid Membrane" @default.
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• W1971242034 doi "https://doi.org/10.1021/ac8008687" @default.
• W1971242034 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/18613700" @default.
• W1971242034 hasPublicationYear "2008" @default.
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