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- W1971292457 abstract "Abstract N , N ‐Diethylcarbamates [NbE(O 2 CNEt 2 ) 3 ] (E = O, S) have been prepared in high yields by treating NbOCl 3 or [NbSCl 3 (CH 3 CN) 2 ] with CO 2 /NHEt 2 in toluene at approximately –10 °C. The products were characterized by spectroscopic techniques, elemental analysis and X‐ray diffractometry in the case of [NbO(O 2 CNEt 2 ) 3 ]. The molecular structure of the latter consists of a niobium centre coordinated to the oxido moiety and six O atoms belonging to bridging and bidentate carbamates, in a slightly distorted pentagonal‐bipyramidal arrangement. The structures of both [NbE(O 2 CNEt 2 ) 3 ] compounds were reproduced by DFT calculations, which show substantial similarity despite the different nature of the chalcogen atoms." @default.
- W1971292457 created "2016-06-24" @default.
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- W1971292457 date "2013-04-26" @default.
- W1971292457 modified "2023-10-16" @default.
- W1971292457 title "Oxido‐ and Sulfidoniobium(V) <i>N</i> , <i>N</i> ‐Diethylcarbamates: Synthesis, Characterization and DFT Study" @default.
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- W1971292457 doi "https://doi.org/10.1002/ejic.201300219" @default.
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