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- W1971319041 abstract "The atomic pair distribution function (PDF) method was used to study the structure of cesium aluminosilicate geopolymer (Cs2O·Al2O3·4SiO2·xH2O, with x ∼ 11). The geopolymer was prepared by reacting metakaolin with cesium silicate solution followed by curing at 50 °C for 24 h in a sealed container. Heating of Cs-geopolymer above 1000 °C resulted in formation of crystalline pollucite (CsAlSi2O6). PDF refinement of the pollucite phase formed displayed an excellent fit over the 10−30 Å range when compared with a cubic pollucite model. A poorer fit was attained from 1−10 Å due to an additional amorphous phase present in the heated geopolymer. On the basis of PDF analysis, unheated Cs-geopolymer displayed structural ordering similar to pollucite up to a length scale of ∼9 Å, despite some differences. Our results suggest that hydrated Cs+ ions were an integral part of the Cs-geopolymer structure and that most of the water present was not associated with Al-OH or Si-OH bonds." @default.
- W1971319041 created "2016-06-24" @default.
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- W1971319041 date "2008-06-18" @default.
- W1971319041 modified "2023-10-02" @default.
- W1971319041 title "Atomic Structure of a Cesium Aluminosilicate Geopolymer: A Pair Distribution Function Study" @default.
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- W1971319041 doi "https://doi.org/10.1021/cm703369s" @default.
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