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• W1971430876 abstract "The compound [W(N)(O-2,6-C6H3iPr2)3]2 has been studied by single-crystal X-ray diffraction (triclinic, P1, a = 12.880(2) Å, b = 14.103(4) Å, c = 20.317(4) Å, α = 90.63(2)°, β = 90.72(2)°, γ= 113.82(2)°, Z = 2). The structure exhibits the first example of an asymmetric, cyclic M2N2 core, with bond orders that alternate between ca. 3 for the short WN linkage (d(WN = = 1.77 Å) and ca. 1 for the longer one (d(WN = 2.02 Å). The 1H HMR spectrum of the compound suggests that the asymmetric, cyclic structure is maintained in solution. This structure represents the fourth spectrum of the compound suggexst that the asymmetric, cyclic structure is steric factors appear to play a significant role in favoring the observed structure." @default.
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• W1971430876 date "1996-02-01" @default.
• W1971430876 modified "2023-09-23" @default.
• W1971430876 title "Molecular structure of [W(N)(O-2,6-C6H3iPr2)3]2: a metal-nitrido compound with a cyclic diyne structure" @default.
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• W1971430876 doi "https://doi.org/10.1016/0020-1693(96)04905-5" @default.
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