Matches in SemOpenAlex for { <https://semopenalex.org/work/W1971555810> ?p ?o ?g. }
- W1971555810 endingPage "156" @default.
- W1971555810 startingPage "150" @default.
- W1971555810 abstract "In arson attacks, accelerants such as ignitable liquids are commonly used to initiate or accelerate a fire. The detection of ignitable liquid residues at fire scenes is therefore a key step in fire investigations. The most widely used analytical technique for the analysis of accelerants is GC–MS. However, pre-concentration of the ignitable liquid residues is required prior to the chromatographic analysis. The standard method, ASTM E1412, involves passive headspace concentration with activated charcoal strips as a method to isolate the ignitable liquid residues from fire debris and these residues are subsequently desorbed from the carbon strip with solvents such as carbon disulfide. In the work described here, an alternative analytical technique based on an HS–MS (headspace mass spectrometry) has been developed for the thermal desorption of the carbon strips and analysis of different ignitable liquid residues in fire debris. The working conditions for the HS–MS analytical procedure were optimized using different types of fire debris (pine wood burned with gasoline and diesel). The optimized variables were desorption temperature and desorption time. The optimal conditions were 145 °C and 15 min. The optimized method was applied to a set of fire debris samples. In order to simulate post burn samples several accelerants (gasoline, diesel, citronella, kerosene, paraffin, and alcohol) were used to ignite different substrates (wood, cotton, cork, paper, and paperboard). chemometric methods (cluster analysis and discriminant analysis) were applied to the total ion spectrum obtained from the MS (45–200 m/z) to discriminate between the burned samples according to the accelerant used. The method was validated by analyzing all samples by GC–MS according to the standard methods ASTM E1412 and ASTM E1618. The results obtained on using the method developed in this study were comparable to those obtained with the reference method. However, the newly developed HS–MS method is faster, safer, and more environmental friendly than the standard method." @default.
- W1971555810 created "2016-06-24" @default.
- W1971555810 creator A5029589911 @default.
- W1971555810 creator A5041558768 @default.
- W1971555810 creator A5044410104 @default.
- W1971555810 creator A5089131860 @default.
- W1971555810 date "2015-09-01" @default.
- W1971555810 modified "2023-10-18" @default.
- W1971555810 title "Application of an HS–MS for the detection of ignitable liquids from fire debris" @default.
- W1971555810 cites W1964170480 @default.
- W1971555810 cites W1970632858 @default.
- W1971555810 cites W1979336564 @default.
- W1971555810 cites W1984142392 @default.
- W1971555810 cites W1996010978 @default.
- W1971555810 cites W1998960802 @default.
- W1971555810 cites W1999439784 @default.
- W1971555810 cites W1999863017 @default.
- W1971555810 cites W2002776107 @default.
- W1971555810 cites W2006068980 @default.
- W1971555810 cites W2029384934 @default.
- W1971555810 cites W2052155501 @default.
- W1971555810 cites W2052194309 @default.
- W1971555810 cites W2052936258 @default.
- W1971555810 cites W2054341846 @default.
- W1971555810 cites W2060420173 @default.
- W1971555810 cites W2063927048 @default.
- W1971555810 cites W2064953900 @default.
- W1971555810 cites W2069543215 @default.
- W1971555810 cites W2073173302 @default.
- W1971555810 cites W2085027329 @default.
- W1971555810 cites W2095413792 @default.
- W1971555810 cites W2101103476 @default.
- W1971555810 cites W2110415417 @default.
- W1971555810 cites W2114054737 @default.
- W1971555810 cites W2114927005 @default.
- W1971555810 cites W2124963039 @default.
- W1971555810 cites W2165899560 @default.
- W1971555810 cites W2172212990 @default.
- W1971555810 cites W2409290837 @default.
- W1971555810 doi "https://doi.org/10.1016/j.talanta.2015.04.030" @default.
- W1971555810 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/26003705" @default.
- W1971555810 hasPublicationYear "2015" @default.
- W1971555810 type Work @default.
- W1971555810 sameAs 1971555810 @default.
- W1971555810 citedByCount "25" @default.
- W1971555810 countsByYear W19715558102016 @default.
- W1971555810 countsByYear W19715558102017 @default.
- W1971555810 countsByYear W19715558102018 @default.
- W1971555810 countsByYear W19715558102019 @default.
- W1971555810 countsByYear W19715558102020 @default.
- W1971555810 countsByYear W19715558102021 @default.
- W1971555810 countsByYear W19715558102022 @default.
- W1971555810 crossrefType "journal-article" @default.
- W1971555810 hasAuthorship W1971555810A5029589911 @default.
- W1971555810 hasAuthorship W1971555810A5041558768 @default.
- W1971555810 hasAuthorship W1971555810A5044410104 @default.
- W1971555810 hasAuthorship W1971555810A5089131860 @default.
- W1971555810 hasBestOaLocation W19715558102 @default.
- W1971555810 hasConcept C103697071 @default.
- W1971555810 hasConcept C127413603 @default.
- W1971555810 hasConcept C138171918 @default.
- W1971555810 hasConcept C150394285 @default.
- W1971555810 hasConcept C162356407 @default.
- W1971555810 hasConcept C162711632 @default.
- W1971555810 hasConcept C178790620 @default.
- W1971555810 hasConcept C185592680 @default.
- W1971555810 hasConcept C2776634852 @default.
- W1971555810 hasConcept C2781059571 @default.
- W1971555810 hasConcept C43617362 @default.
- W1971555810 hasConcept C77595967 @default.
- W1971555810 hasConceptScore W1971555810C103697071 @default.
- W1971555810 hasConceptScore W1971555810C127413603 @default.
- W1971555810 hasConceptScore W1971555810C138171918 @default.
- W1971555810 hasConceptScore W1971555810C150394285 @default.
- W1971555810 hasConceptScore W1971555810C162356407 @default.
- W1971555810 hasConceptScore W1971555810C162711632 @default.
- W1971555810 hasConceptScore W1971555810C178790620 @default.
- W1971555810 hasConceptScore W1971555810C185592680 @default.
- W1971555810 hasConceptScore W1971555810C2776634852 @default.
- W1971555810 hasConceptScore W1971555810C2781059571 @default.
- W1971555810 hasConceptScore W1971555810C43617362 @default.
- W1971555810 hasConceptScore W1971555810C77595967 @default.
- W1971555810 hasFunder F4320325313 @default.
- W1971555810 hasLocation W19715558101 @default.
- W1971555810 hasLocation W19715558102 @default.
- W1971555810 hasLocation W19715558103 @default.
- W1971555810 hasOpenAccess W1971555810 @default.
- W1971555810 hasPrimaryLocation W19715558101 @default.
- W1971555810 hasRelatedWork W1976303652 @default.
- W1971555810 hasRelatedWork W2016227923 @default.
- W1971555810 hasRelatedWork W2316689885 @default.
- W1971555810 hasRelatedWork W2339744400 @default.
- W1971555810 hasRelatedWork W2367341701 @default.
- W1971555810 hasRelatedWork W2367904106 @default.
- W1971555810 hasRelatedWork W2386446702 @default.
- W1971555810 hasRelatedWork W2522878691 @default.
- W1971555810 hasRelatedWork W3146526220 @default.
- W1971555810 hasRelatedWork W3214447609 @default.