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• W1971595449 abstract "The thiol–ene reaction serves as a more oxygen-tolerant alternative to traditional (meth)acrylate chemistry for forming photopolymerized networks with numerous desirable attributes including energy absorption, optical clarity, and reduced shrinkage stress. However, when utilizing commercially available monomers, many thiol–ene networks also exhibit decreases in properties such as glass transition temperature (Tg) and cross-link density. In this study, hybrid organic/inorganic thiol–ene resins incorporating silsesquioxane (SSQ) species into the photopolymerized networks were investigated as a route to improve these properties. Thiol- and ene-functionalized SSQs (SH-SSQ and allyl-SSQ, respectively) were synthesized via alkoxysilane hydrolysis/condensation chemistry, using a photopolymerizable monomer [either pentaerythriol tetrakis(3-mercaptopropionate) (PETMP) or 1,3,5-triallyl-1,3,5-triazine-2,4,6(1H,3H,5H)-trione (TATATO)] as the reaction solvent. The resulting SSQ-containing solutions (SSQ-PETMP and SSQ-TATATO) were characterized, and their incorporation into photopolymerized networks was evaluated." @default.
• W1971595449 created "2016-06-24" @default.
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• W1971595449 date "2011-09-15" @default.
• W1971595449 modified "2023-09-26" @default.
• W1971595449 title "Hybrid Organic/Inorganic Thiol–Ene-Based Photopolymerized Networks" @default.
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• W1971595449 doi "https://doi.org/10.1021/ma201695x" @default.
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