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- W1971624476 abstract "3H-Labelled ubenimex, N- (2S,3R)-3-amino-2-hydroxy-4-(o-3H)phenylbutyrl)-S-leucine with a specific radioactivity of 15 mCi/mg was synthesized by a one step catalytic tritiation of N- ((2S,3R)-3-benzyloxycarbonylamino-2-hydroxy-4-(o-bromo)phenylbutyryl)-S-leucine benzyl ester previously isolated from a mixture of four optical isomers using preparative high performance liquid chromatography.Chemical and radiochemical purities were over 99% as determined by thin layer chromatography and high performance liquid chromatography using radioisotope detection. By gas chromatography-mass spectrometric analysis of deuterated ubenimex, the 3H-label was determined to be in the aromatic ring." @default.
- W1971624476 created "2016-06-24" @default.
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- W1971624476 date "1988-12-01" @default.
- W1971624476 modified "2023-09-24" @default.
- W1971624476 title "A simple synthesis of 3H-labelled ubenimex" @default.
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- W1971624476 doi "https://doi.org/10.1002/jlcr.2580251202" @default.
- W1971624476 hasPublicationYear "1988" @default.
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