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- W1972222179 abstract "Abstract Polymer‐derived amorphous Si–C–N ceramics are phase separated into amorphous nanodomains after thermolysis. These nanodomains are expected to have a crucial importance for the extraordinary high temperature stability of these materials. We investigated nanodomain growth during isothermal annealing at 1400 °C using small angle X‐ray scattering. The as‐thermolyzed sample shows a domain radius of about 5 Å as determined from Guinier plots. During annealing, fast nanodomain growth up to 9 Å is observed for times up to 30 h while for longer annealing times up to 165 h the growth considerably slows down, resulting in a domain size of 11 Å. The experimental data can be fitted by a model based on diffusion controlled domain growth and simultaneous slow‐down of diffusion due to structural relaxation. (© 2009 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim)" @default.
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- W1972222179 date "2009-03-01" @default.
- W1972222179 modified "2023-10-16" @default.
- W1972222179 title "Nanodomain growth in amorphous Si-C-N" @default.
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- W1972222179 doi "https://doi.org/10.1002/pssr.200903012" @default.
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