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- W1972231346 abstract "Several structural analogs of prednisolone, prepared by esterification of the carboxylic and/or the C(17)-hydroxy group of 11β,17α-dihydroxy-3-oxo-androsta-1,4-diene-17β-carboxylic acid, were investigated by NMR. Step-by-step analysis of the 1H and 13C NMR spectra of these steroids, including proton-proton selective decoupling, nuclear Overhauser effect difference spectra, attached proton test, proton-carbon correlation (HETCOR), proton-proton correlation (COSY), and long-range proton-carbon decoupling (INAPT) techniques, led to unequivocal assignments of all their proton and carbon resonances. The stereochemical structure of loteprednol etabonate (chloromethyl 17α-ethoxycarbonyloxy-11β-hydroxy-3-oxoandrosta-1,4-diene-17β-carboxylate, 1), a soft corticosteroid antiinflammatory drug, was proved to be analogous to prednisolone." @default.
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- W1972231346 date "1996-09-01" @default.
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- W1972231346 title "Structural studies of loteprednol etabonate and other analogs of prednisolone using NMR techniques" @default.
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- W1972231346 doi "https://doi.org/10.1016/s0039-128x(96)00090-6" @default.
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