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- W1972332364 abstract "1,2,3,4-Tetra-O-acetyl-5-thio-D-xylopyranose (1) reacts with the silylated lumazine bases (2–5) under trimethylsilyl trifluoromethylsulfonate catalysis to give the nucleosides 6, 8, 10, and 12 respectively, which face deblocking with potassium carbonate in dry methanol to yield the free nucleosides 17, 9, 11, and 13 respectively. The synthesis of 1-(2,3,4-tri-O-acetyl-5-thio-β-xylopyranosyl)-thymine (17) and its free nucleoside 18 have been improved and in a similar manner reacted the silylated pyrimidine bases 15 and 16 to the 5-iodo- (19) and 5-fluoro- (21) analogues. Deacylation afforded the free nucleosides 20 and 22, respectively." @default.
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- W1972332364 date "1993-08-01" @default.
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- W1972332364 title "Synthesis of some novel 1-(5-thio-β-D-xylopyranosyl)-lumazine and -pyrimidine nucleosides" @default.
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- W1972332364 doi "https://doi.org/10.1016/s0040-4020(01)87232-x" @default.
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