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- W1972673825 abstract "A comprehensive mass fragmentation of linezolid, which was not been reported so far, was established by subjecting the drug to liquid chromatography/mass spectrometric (LC-MS) analysis and multi-stage mass spectrometric studies. The objective of the present investigation was to separate, identify, and characterize all the degradation products (DPs) of linezolid, generated under various stress conditions. The drug was subjected to hydrolytic, oxidative, photolytic, and thermal stress as per International Conference on Harmonization (ICH) guideline Q1A(R2). The drug was found to be labile under acidic, basic, neutral, and oxidative stress while it was stable in photolytic and thermal stress conditions. A total of three degradation products were formed, which were separated on a C-18 column employing a gradient high-performance liquid chromatographic (HPLC) method. A complete mass fragmentation pathway of the drug was first established with the help of multi-stage (MSn) and MS/TOF accurate mass studies. Then..." @default.
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- W1972673825 date "2012-01-01" @default.
- W1972673825 modified "2023-10-17" @default.
- W1972673825 title "LC, LC–MS/TOF, AND MSN STUDIES FOR THE SEPARATION, IDENTIFICATION, AND CHARACTERIZATION OF DEGRADATION PRODUCTS OF LINEZOLID" @default.
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- W1972673825 doi "https://doi.org/10.1080/10826076.2011.597069" @default.
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