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- W1973002259 abstract "A copolyester was characterized to have 91 mol% trimethylene terephthalate unit and 9 mol% ethylene terephthalate unit in a random sequence by using 13C NMR. Differential scanning calorimeter (DSC) was used to investigate the isothermal crystallization kinetics in the temperature range (Tc) from 180 to 207 °C. The melting behavior after isothermal crystallization was studied by using DSC and temperature modulated DSC (TMDSC). The exothermic behavior in the DSC and TMDSC curves gives a direct evidence of recrystallization. No exothermic flow and fused double melting peaks at Tc = 204 °C support the mechanism of different morphologies. The Hoffman–Weeks linear plot gave an equilibrium melting temperature of 236.3 °C. The kinetic analysis of the growth rates of spherulites and the morphology change from regular to banded spherulites indicated that there existed a regime II → III transition at 196 °C." @default.
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- W1973002259 date "2007-04-01" @default.
- W1973002259 modified "2023-09-30" @default.
- W1973002259 title "Poly(trimethylene terephthalate) copolyester containing ethylene glycol moieties. Part 1: Crystallization kinetics and melting behavior" @default.
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- W1973002259 doi "https://doi.org/10.1016/j.polymer.2007.02.042" @default.
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