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- W1973104948 abstract "Abstract The systems C 5 H 5 NBBr 2 CH 3 , C 5 H 5 NBBr(CH 3 ) 2 , 4-CH 3 C 5 H 4 NBBr 2 CH 3 , 4-CH 3 C 5 H 5 NBBr(CH 3 ) 2 , (CH 3 ) 3 NBBr 2 CH 3 , (CH 3 ) 3 NBBr(CH 3 ) 2 , (CH 3 ) 3 PBBr 2 CH 3 and (CH 3 ) 3 PBBr(CH 3 ) 2 are reported. The bromomethylboranes are not available commercially and, therefore, were synthesized as required. All of the systems were found to form 1:1 adducts except pyridine and 4-methylpyridine which form only 2:1 adducts with bromodimethylborane, i.e. (C 5 H 5 N) 2 BBr(CH 3 ) 2 and (4-CH 3 C 5 H 4 N) 2 BBr(CH 3 ) 2 . These systems were studied and characterized by tensimetric titrations, IR spectroscopy, 11 B and 1 H NMR spectroscopy, elemental analyses, vapor pressure determinations, molecular weight determination, and m.p. determinations as appropriate." @default.
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- W1973104948 date "1978-01-01" @default.
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- W1973104948 title "Dibromomethylborane and bromodimethylborane adducts with pyridine, 4-methylpyridine, trimethylamine and trimethylphosphine" @default.
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- W1973104948 doi "https://doi.org/10.1016/0022-1902(78)80036-0" @default.
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