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- W1973259743 abstract "The sequential reaction of selected polycyclic aromatic hydrocarbons with butyllithium/TMEDA/hexane and sulfur allows preparation of ring-fused dithiins, dithioles, and thiophenes. In this manner, phenanthrene has been converted to phenanthro[4,5-cde][1,2]dithiin and phenanthro[1,10cd]-1,2-dithiole. Yellow crystals of the dithiin form in C2/c (#15) space group with Z = 4, a = 13.537(3) Å, b = 8.933(2) Å, c = 9.601(4) Å, and β = 116.19 (2)°; while orange crystals of the dithiole form in P212121 (#19) space group with Z = 4, a = 4.1507(5) Å, b = 14.436(3) Å, and c = 16.972(3) Å. Full structures have been determined for both compounds." @default.
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- W1973259743 date "1994-04-01" @default.
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- W1973259743 title "The reaction of sulfur with dilithio compounds. The syntheses and structures of phenanthro [1, 10-cd]-1,2-dithiole and phenanthro[4,5-cde] [1,2]dithiin" @default.
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- W1973259743 doi "https://doi.org/10.1002/hc.520050206" @default.
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