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- W1973289814 abstract "The symmetry transformation of aluminophosphate molecular sieve AlPO4-31 and the interaction of its framework with dipropylamine template molecules were studied by variable temperature XRD and multinuclear MAS, CPMAS, and MQMAS NMR measurements. The as-synthesized material exhibited triclinic symmetry with a slightly distorted rhombohedral-like unit cell. Deviation from a rhombohedral symmetry was due to a large amount of template within cavities of a molecular sieve, which caused short contacts with the aluminophosphate framework. The template within AlPO4-31 was in the form of dipropylammonium hydroxide ionic pairs, whose arrangement did not possess a long-range order. Hydroxyl groups, not being isolated by surrounding alkyl groups, interacted with the aluminophosphate framework and gave rise to 5-coordinated aluminum sites. Dipropylammonium and hydroxyl groups were also coupled to the framework through hydrogen bonds with the framework oxygen and affected the local environments of the 4-coordinated alu..." @default.
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- W1973289814 date "2001-12-05" @default.
- W1973289814 modified "2023-10-15" @default.
- W1973289814 title "Interaction of Dipropylamine Template Molecules with the Framework of as-Synthesized AlPO4-31" @default.
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- W1973289814 doi "https://doi.org/10.1021/jp012942b" @default.
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